INVESTIGATION OF MASS GRADIENT OF CONCRETE FILLED WITH POLYACRYLAMIDE/Fe3O4 MAGNETITE NANOPARTICLES İN CASPIAN SEA AND FORMATION WATER MEDIUM

S.F. Humbatova, Sh.Z. Tapdyqov, J.E. Guliyeva, A.M. Gulamirov, E.Y. Malikov, S.M. Mammadova, A.A. Fariz, S.Sh. Kazimova

Abstract

In the study, changes in the mass of concrete filled with polyacrylamide/Fe3O4 nanoparticles in an amount of 1–2% of the cement mass in sea and formation water were studied. Besides, by performing IR and X-ray characterization of the prepared samples, the chemical state of the polyacrylamide (PAA) and the nanoparticles in the structure was also determined. Changes in mass of concrete samples containing PAA/Fe3O4 nanoparticles in highly mineralized seawater were shown to be highly dependent on the amount of nanoparticles compared to PAA. It revealed that at 2% PAA-Fe3O4/concrete, the ion penetration was limited and there was a lower weight gain as compared to the control concrete. IR spectroscopic analyses proved that the polymer was in a coordination band with cement and magnetite nanoparticles. X-ray diffraction studies showed a slight increase in the crystallinity of the concrete filled with up to 2% PAA/Fe3O4 magnetite nanoparticles.

https://doi.org/10.32737/2221-8688-2024-1-95-102